Optical and structural analysis of the MgFe2O4 nanoparticles, synthesized by the solid-state reaction of inorganic precursor route.

Mrityunjay Kumar Mishra , Bibhuti Shekhar Lal Das , Sujit Kumar

Solid-state reaction of inorganic precursor method, FTIR, XRD, Raman spectroscopy, Magnesium ferrite, FESEM

In this study the result obtained from different characterizations for the MgFe2O4 nanoparticles by solid state reaction of inorganic precursor’s technique. Structural properties are carried out by using X-ray diffraction (XRD) technique and then formation of spinel MgFe2O4 structure is confirmed by Fourier transform infrared spectroscopy (FTIR). The XRD of the powder sample was done at room temperature which gives the lattice parameter of the sample. The cations distribution is also confirmed by IR spectroscopy and Raman spectroscopy. An FTIR spectrum of the calcined samples at 800 c, gives the two strong absorption bands (ѵ1 and ѵ2) which are the characteristic bands of the spinel MgFe2O4. The ѵ1 is high band due to the stretching vibrations of the Mg and O bonds in tetrahedral site while the low band ѵ2 is appeared due to the bending vibration of the Mg-O bonds in octahedral site, these bands are appeared due to the different bond lengths in each sites. The local deformation takes place due to the presence of Fe2+ cations at octahedral site, known as Jahn-Teller effect. The morphology of the nanoparticles is observed by ZEISS field emission scanning electron microscopy at BIT Meshra.

Published Paper   E-Certificate

"Optical and structural analysis of the MgFe2O4 nanoparticles, synthesized by the solid-state reaction of inorganic precursor route.", IJSDR - International Journal of Scientific Development and Research (www.IJSDR.org), ISSN:2455-2631, Vol.8, Issue 3, page no.372 - 376, March-2023, Available :https://ijsdr.org/papers/IJSDR2303058.pdf

Volume 8 Issue 3, March-2023

Pages : 372 - 376

Paper Reg. ID: IJSDR_204393

Published Paper Id: IJSDR2303058

Downloads: 000347523

Research Area: Physics

Country: Samastipur , Bihar, India

Published Paper PDF: https://ijsdr.org/papers/IJSDR2303058

Published Paper URL: https://ijsdr.org/viewpaperforall?paper=IJSDR2303058

ISSN: 2455-2631 | IMPACT FACTOR: 9.15 Calculated By Google Scholar | ESTD YEAR: 2016

An International Scholarly Open Access Journal, Peer-Reviewed, Refereed Journal Impact Factor 9.15 Calculate by Google Scholar and Semantic Scholar | AI-Powered Research Tool, Multidisciplinary, Monthly, Multilanguage Journal Indexing in All Major Database & Metadata, Citation Generator

Publisher: IJSDR(IJ Publication) Janvi Wave

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