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INTERNATIONAL JOURNAL OF SCIENTIFIC DEVELOPMENT AND RESEARCH International Peer Reviewed & Refereed Journals, Open Access Journal ISSN Approved Journal No: 2455-2631 | Impact factor: 8.15 | ESTD Year: 2016 open access , Peer-reviewed, and Refereed Journals, Impact factor 8.15 |
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| Paper Title: | Metho development of umbralisib by using RP HPLC |
| Authors Name: | K Hima Bindu , Dr. K. Venkataramana , K. Kalyan Chakravarthi |
| Unique Id: | IJSDR2307107 |
| Published In: | Volume 8 Issue 7, July-2023 |
| Abstract: | A simple, rapid, precise, sensitive and reproducible reverse phase high performance liquid chromatography (RP-HPLC) method has been developed for the quantitative analysis of Umbralisib in pharmaceutical dosage form. Chromatographic separation of Umbralisib was achieved on Waters Alliance-e2695, by using Waters X-Terra RP-18 Column (150x4.6mm, 3.5µ) column and the mobile phase containing ACN and Ammonium formate pH-3.0/OPA in the ratio of 50:50% v/v. The flow rate was 1.0 ml/min; detection was carried out by absorption at 225nm using a photodiode array detector at ambient temperature. The number of theoretical plates and tailing factor for Umbralisib were NLT 2000 and should not more than 2 respectively. % Relative standard deviation of peak areas of all measurements always less than 2.0. The proposed method was validated according to ICH guidelines. The method was found to be simple, economical, suitable, precise, accurate & robust method for quantitative analysis of Umbralisib. |
| Keywords: | HPLC Umbralisib |
| Cite Article: | "Metho development of umbralisib by using RP HPLC", International Journal of Science & Engineering Development Research (www.ijsdr.org), ISSN:2455-2631, Vol.8, Issue 7, page no.745 - 750, July-2023, Available :http://www.ijsdr.org/papers/IJSDR2307107.pdf |
| Downloads: | 000338536 |
| Publication Details: | Published Paper ID: IJSDR2307107 Registration ID:207681 Published In: Volume 8 Issue 7, July-2023 DOI (Digital Object Identifier): Page No: 745 - 750 Publisher: IJSDR | www.ijsdr.org ISSN Number: 2455-2631 |
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